TopSizer Laser Particle Size Analyzer

——leading role in China

TopSizer is a high-performance Laser particle analyzer that OMEC developed it with 20 years profound research and development experience .its advantages contain wide measurement range, good repeatability, high accuracy, true test result and high reliability. Now OMEC represents the most advanced technology in the China test and analysis area. And always represents the leader role in particle test area.

 
Technical instruction:

1.      Measure rang:0.02～2000μm(wet), 0.1～2000μm (dry)

2.      Theory: Mie theory

3.      Repeatability : ≤0.5%(standard particle D50)

         Accuracy : ≤±0.6 %( standard particle D50)

4.      Test speed: within 10 second for common sample

5.      Sampling way: wet and circulating test( water and organic solvent)

Adopt the advanced circulation loop design and big power precise centrifugal pump, the stirring speed can reach 4000turn /min, with the advantage of efficiency clean ability and unwater ability. The inserted inside ultrasonic can reach 100W. Contain 1000ML sampler, customer can change the volume of the sampler according to their need.

6.      Light path system:

Red lightis imported He-Ne laser with 0.6328μm wavelength；and solid blue laser with 0.466μm wavelength，it improve the resolution ratio of the nanometer particle and big particle. The powder is stable, and fluctuation of powder is less than 0.5%

The designcomply with the international laser safety principle, and capable of self-protection function

The light pathadopts the folding light path design, the structure is compact and artistic, and it was made of high accuracy aluminum alloy light stage to insure the light path is steady and reliable.

Single lens design, adopt the structure of lens back Fourier change, and break the restrict the pupil of the Fourier lens, and insure the maximum acceptance angle won’t be restricted by the Fourier lens caliber; And help to keep the reflector and refractor to the lowest situation, moreover it helps to decrease the background noise to the lowest standard, all in all the sensitivity will be raised. And the light path system is closed, it is effective to get rid of contaminate.

7.      Detector:

The detective path reach 98 pieces, and its forward direction, side direction, big angle and backward direction photoelectric detector make up the three-dimensional system, the big detective angle is 140°，the small detective angle is 0.016°.

8.      Software function:

Software design modularization, invisible instrument state, humanized operation interface.

SOP standardization operating procedure

Different date analysis mode, fulfill the measure need of different characterized sample

Clear navigation function and flow interface

Contain the artificially intelligent, and instrument self-check function, and automatic

distinguish the sample injector. And automatic measure the background before testing.

Lots of way to derive the data, convenient to transfer the data.

Comprehensive and open sample character parameter data base, and contain the sample refractive index and absorptivity index

Manual transformation among volume distribution, superficial area distribution, length distribution and number distribution

9.      Dimension；

Mainframe：1310×275×425mm

Circulated sample feeding system: 265×325×405mm（SCF-108），210×260×345mm（SCF-105B）

Dry-dispersion sample feeding system: 305×245×295mm（DPF-110）

1. Application: measure the particle distribution of the powder and latex

2. Theory: Light is an electromagnetic wave. When light meets with particles on it way of traveling, the interaction between light and particles will result in deviations of part of the light, which is called light scattering. The bigger the scattering angle is, the particle size will be smaller, the smaller the scattering angle is, the particle size will be bigger. The particle analyzer instruments will analysis the particle distribution According to this physical character of the light wave.

3. Advance light system

Double light resource skill  

TopSizer adopts double light resource skill. Red light is imported He-Ne laser with 0.6328μm wavelength；and solid blue laser with 0.466μm wavelength，it improve the resolution ratio of the nanometer particle and big particle.OMEC is one of the companies that adopt this double light resource skill in China.  

Stable laser resource  

Short preheat time. The output ratio of dual-polarization laser is 500:1，and the ratio of TEM00  reach  

95%, the powder is stable, and fluctuation of powder is less than 0.5%, it helps to keep the background of  

The instrument in a low and stable state, and largely improve the resolution ratio of the system.  

Folding light path design  

The light path of the TopSizer adopts the folding light path design, the structure is compact and artistic, and it was made of high accuracy aluminum alloy light stage to insure the light path is steady and reliable.  

Single lens design  

Single lens design, adopt the structure of lens back Fourier change, and break the restrict the pupil of the Fourier lens, and insure the maximum acceptance angle won’t be restricted by the Fourier lens caliber; and  

help to keep the reflector and refractor to the lowest situation, moreover it helps to decrease the background noise to the lowest standard ,all in all the sensitivity will be raised.   

Long-focus Fourier lens  

TopSizer adopts the long-focus Fourier lens, it helps to add the distance between the test window and photoelectric detector(the effective distance), and insure the  photoelectric detector can accept the signal of the smallest scattering angle accurately, and strengthens the capability of measuring the big particle, the upper limit can reaches 2000μm.   

Reasonable and high-sensitivity of the exported photoelectric detector  

TopSizer adopts the special customized exported photoelectric detector, which insures the high resolution ratio and sensitivity of the instrument. The detective path reach 98 pieces, and its forward direction, side direction, big angle and backward direction photoelectric detector make up the three-dimensional system, the big detective angle is 140°，the small detective angle is 0.016°,combine the solid blue scatter signal, insure the detector will accept the signal from the whole space without omit, and the information of the particle scattering can be captured.  

Intelligent automatic centering  

The intelligent software control system insures the accurate optical centering. Automatic centering will be finished within several seconds, this operation can be completed as a part of the automatic measurement, or you can kick the monitor to finish. This automatic insures the repeatability of the instrument.  

Excellent dispersing system  

Wet dispersion: standard configuration SCF-108, adopt the advanced circulation loop design and big power precise centrifugal pump, the stirring speed can reach 4000turn /min, with the advantage of efficiency clean ability and unwater ability. The inserted inside ultrasonic can reach 100W. Contain 1000ML sampler, customer can change the volume of the sampler according to their need. SCF-105B fully automatic circulating sample feeding system can be selected, all test operation can be automatically controlled except for adding samples. The sampling tank is made of 316L stainless steel, equipped with a precision mixing device with a high efficiency of 50W bottom ultrasonic and a speed of 4000 rpm, all of which can be continuously adjusted.  

Dry dispersion: standard configuration DPF-110 automatic dry sample feeding system with stepless adjustable, dispersion pressure of 0.05-0.6 MPa and triple adjustable cutting mechanism is designed to meet the requirements of various sample testing for dispersion strength. Built-in pressure sensor and negative pressure sensor, test window is fully closed, with negative pressure protection device, can effectively prevent window and host pollution.  

Powerful analysis software   

Software design modularization, invisible instrument state, humanized operation interface.  

Clear navigation function and flow interface.  

The instrument has intelligent and automatic operation. It can self-check and automatically identify the sample feeding system, automatically measure the background before each measurement, effectively eliminate the influence of electrical noise on the test results. Automated sample feeder can be equipped for automatic dry & wet particle size measurement, manual sampling also has clear navigation testing function.  

Perfect and open database of sample characteristic parameters with common refractive index and absorptivity parameters
SOP standard operation process, reduce the influence of human factors, standardize analysis and testing process
SOP measurement control interface:

When the instrument is equipped with a wet automatic sampler (SCF-105B), the upper left figure is the control panel of the wet sampler. Users can set pump speed, ultrasonic power, timing ultrasound time, turn on and off timing ultrasound, and can perform water intake, exhaust bubbles, cleaning, drainage and stop operations.
Automatic Sampler Control Panel

When the instrument is equipped with dry automatic sampler (DPF-110),  the control panel of the dry sampler on the upper right can set the  feeding rate, select the air flow control mode, and perform automatic  cleaning and stopping operations.When the instrument is equipped with  dry automatic sampler (DPF-110), the control panel of the dry sampler on  the upper right can set the feeding rate, select the air flow control  mode, and perform automatic cleaning and stopping operations.

When the instrument is equipped with wet-dispersion sample feeding system (SCF-105B), the upper left figure is the control panel of the sample feeder. Users can set pump speed, ultrasonic power, timing ultrasound time, turn on and off timing ultrasound, and can perform water intake, exhaust bubbles, cleaning, drainage and stop operations.  

When the instrument is equipped with dry-dispersion sample feeding system (DPF-110), the control panel of the sample feeder on the upper right can set the feeding rate, select the air flow control mode, and perform automatic cleaning and stopping operations.

  

Different date analysis mode, fulfill the measure need of different characterized sample.  

Volume distribution, surface area distribution, length distribution and quantity distribution can be converted to each other.

Lots of way to derive the data, convenient to transfer the data.

Compatible with the requirements of CFDA/FDA cGMP 21CFR for user classification, authority management, data integrity and traceability  

5. Charming instrument performance  

Wide measurement range   

TopSizer measurement rang is from 0.02μm to 2000μm，which could test from submicron to millimeter in one sample, it can meet all kinds of requirements for particle size measurement and control in powder industry.  

Powerful test performance for large particles

750-1600um glass beads

Good recognition capability for the nanometer and submicron particle  

Good repeatability
TopSizer uses automatic laser calibration system and automatic alignment  system, which ensures the accuracy of laser angle calibration, avoids  the drift of optical path, and ensures that the repeatability error of  the test is less than 0.5% (standard particle D50).

Excellent reproducibility   

Be capable of good reproducibility among different main machines and different sample feeding systems  

Intelligent resolution ratio  

Topsizer can distinguish tiny change in the distribution of the sample ,and accurate reflect the real particle distribution for the sample, and sufficient statisfy all the technical research and quality control need. 

Rapid test speed

The initial fast dispersing system provide the condition for fast speed, therefore insure the common test complete within 10S, largely improve the test efficiency and better meet the customers’ demand.  

High sensitivity  

The detective path reach 98 pieces, and its forward direction, side direction, big angle and backward direction photoelectric detector make up the three-dimensional system, the big detective angle is 140°，the software will automatic test the signal noise before measuring, it helps the instruments are sensitive to the little particle.  

Good adaptation  

The dispersing system is capable of dispersing the sample, which insure the dense mental powder and glass powder won’t precipitate, and meet different measure demand for different kinds of dense sample.  

6. Sample feeding system

DPF-110 Automated dry-dispersion sample feeding system  

1. Concise and fluent design, elegant appearance.  

2. Communication recognition between sample feeder and main engine; SOP automated measurement function: automated positive and negative pressure switch, automated feeding, automated sample measuring, automated cleaning.  

3. Dispersive pressure 0.5～6Bar, high-precision stepless control, built-in dispersive pressure sensor.  

4. Automated recognition of dispersion state of samples, automated restriction of beam obscuration, warning anomaly.  

5. Optimized design of sample cell, vibrational frequency is controlled by software, continuously adjustable.  

6. Totally-enclosed sample feeder with noise reduction, protect instrument from being polluted by powders, few maintenance demands.  

7. Maximum volume of hopper：30ml; sampling vibration acceleration: 0~12G stepless control.   

8. Dispersion pipe of sample feeder uses corundum ceramic materials; advantages: good dispersion effects, long life.  

9. Specialized dry-dispersion window, quartz glass material, airflow protection, easy to clean, long service life.  

10. Modular design, convenient for overhauling and maintenance.

         SCF-108 circulating sample feeding system  

Technical features of SCF-108 circulating sample feeding system  

1. SCF-126 can be configured with LS-909. Modular design, operation is convenient.   

2.Use unique centrifugal pump circulating structure of lantern pattern（patent no.: 2012204087053）.  

3. Circulating pump body uses high-quality SU316 stainless steel.  

4. Imported continuous current dynamo with original packing, can realize 600~4000 rpm stepless speed control, has high-efficient cleaning and draining ability.  

5. Built-in 40 KHZ ultrasonic frequency, power is stepless adjustable, maximum power: 100w, ultrasound time: 0 ~ 30 minutes (stepless adjustable)  

6. Use the design of downward water flow dispersion technology, the dispersion effect keeps good even for high-density samples.   

7. Advanced circulation loop design, particles are not easy to drop, the test data can reflect the real character of samples effectively.  

8. Standard configuration of 1000ml sample pool, the capacity can be changed as required.

     SCF-126 micro circulating sample feeding system  

Technical features of SCF-126 circulating sampling system  

1. SCF-126 can be configured with LS-909. Most of the overall structure uses stainless steel.  

2. Small volume for circulation loop and sample cell, it will consume fewer dispersants.  

3. Can be used for the measurement of valuable powder samples.  

4. Sampling system uses centrifugal pump structure, selects imported motor, speed: 450~3500 rpm (stepless speed control).  

5. Use precision potentiometer knob to adjust the motor speed to realize stepless speed regulating.  

6. Speed control circuit owns speed detection module, it can control the rotate speed of water pump accurately.  

7. Use external DC 24V power module for power supply, it can improve the safety factor of system.  

8. The pipeline of sample feeder can resist the corrosion from weak acid and weak base properly.  

9. The user can select the configuration of anti-corrosion, the internal pump body’s sealing ring uses FKM, the external pipeline may use EPDM or FKM.